Synchrotron radiation is a high-performance instrument for many kinds of science and industry now. The increasing interest in this light source opens new possibilities for fundamental and applied researches. Synchrotron Radiation (SR) tools replace researchers into atomic scale world due to extremely small wavelengths of SR and ultra high vacuum chambers. Thus exceedingly stringent specifications are placed on the used optical component. The high heat conductivity and low thermal expansion are necessary for SR substrates (lower deformation) as well as good optical machinability and long-term stability.
The quality of grazing incident optics is accepted to characterize by Surface Figure Error user friendly. This term describes the maximum (PV) or average (RMS) deviation of the actual form from the ideal surface. Since the quality of the focus with grazing incident optics is primarily determinated by the slope distribution on the surface, it is more common to use the RMS Slope Error as a specification for global form accuracy. Typical value is from 0.05 microRad/rms (for flat surface) till 0.1 microRad/rms (aspherical surface). For visual Interferometric inspection is used the shape accuracy as part of test wavelength(pv or rms), e.g. « λ/130(rms)@633nm » - at the test wavelength λ=632.8nm. Interferometric measured technique is best suited for plane and spherical surfaces. Aspherical surfaces can be tested if a component-specific null lens is used. This lens compensates the wavefront aberrations resulting from the aspheric deformation. Micro-Roughness is measured by Microinterferometer or 3D Optical Profiler with resolution of better than 0.1nm, e.g."NewView 5000" Zygo Co.
Typical surface geometry of synchrotoron mirrors
- Flat => ( best slope error is reached);
- Sphere, Cylinder => ( very good slope error);
- Toroids, Elliptic/parabolic cylinder, Elliptical toroid => (good slope error);
- Ellipsoid (rotary), Paraboloid, Hyperboloid; FreeFORM Surface => (good slope error).
Typical mirrors substrate materials
For low SR flux:
- Zerodur®, Astrositall®( Sitall CO-115M)
- Fused Silica
- ULE™
- Glasses (Pyrex, BK7, …)
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For high SR flux:
- Silicon (single crystal)
- Silicon Carbide (CVD)
- Cu with electroless Ni layer
- Al with electroless Ni layer
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Manufacturing Techniques
There are two techniques for SR Mirrors: Direct Manufacturing and Replication by negative masterform.
The direct manufacturing process generally includes the following steps:
- Grinding approaches for pre-manufacturing of substrates and optical surface geometry;
- Etching for reducing stress and subsurface damages;
- Lapping for performing good thermal contact at the side faces and for optimizing the optical
surface for subsequent steps;
- Polishing for correcting and smoothing the surface by several steps.
To achieve the desired quality, a very close interaction between metrology and polishing is necessary. Depending on the type of mirror geometry and on the required accuracy, the fine correction of residual errors has to be performed by:
- conventional polishing; for Plane & Spherical mirrors, rms-Roughness:<2 nm; ~4 Å (Magnetorheological)
- computer controlled fine-correction polishing -tool for high-end figuring of aspherical(<0.1 microRad)
- Ion Beam Figuring - powerful tool for high-end figuring of optical surfaces with any form (<0.1 microRad)
- Metal Mirrors can also be performed by Diamond Turning methods and Replication Technique.
C o a t i n g s
Commonly used coating materials: Au, Pt, Rh, Ni, Pd, Al, Si, Ru, SiO2, Al/MgF2 etc. In some cases (e.g. Ru) a thin Cr binding layer (~0.4
nm) is necessary for reducing stress and also for keeping the microroughness performance. Practically each of coater-producers have “know-how” for Art coatings of Extra UV HR Mirrors. ZILTA offers the “Special EUV HR” (=>Xuv) for lambda < 50
nmtoo. Nominal Reflection for different metallic coating at AOI =75 degree for VUV mirrors (Theoretically, nonpolarized ):
Platinum |
Gold Standard EUV (Au_40nm/ Cr_binder) |
Nickel |
R=60% (55-58%)@200nm -65nm |
R=60% (55-58%)@200nm -65nm |
R=64% (68-60%)@200nm -120nm |
R=66% (60-69%)@ 65nm -27nm |
R=62% (55-65%)@ 65nm -25nm |
R=58% (60-56%)@120nm - 40nm |
R=57% (60-55%)@ 27nm -22nm |
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R=65% (70-60%)@ 41nm - 30nm |
R=62% (60-65%)@ 22nm -12nm |
R=64% (61-70%)@ 25nm -15nm |
R=45% (60-30%)@ 30nm - 20nm |
R=52% (55-50%)@ 12nm -10nm |
R=65% (71-70%)@ 15nm - 9nm |
R=35% (30-40%)@ 20nm - 16nm |
Mirror Reflectivity is calculated using the Fresnel equations for a semi-infinite medium
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